Has anyone dealt with moisture content analysis for lyophilized peptides?

One concrete data point for the thread. Worth stating the units and the reference range whenever you post a number here. A large fraction of the apparent disagreement in these threads is two people using different units and both being right.

One thing that is still open after BariatricNurseD’s answer:

What did you change at the same time, and can you separate the two now?

BethLabQueen said:

Worth stating the units and the reference range whenever you post a number here.

I am going to disagree with the direction of travel here. The thread has converged on the tidiest answer rather than the best-supported one, and those are not the same thing.

I would rather be corrected than agreed with, if it comes to it.

BethLabQueen said:

Worth stating the units and the reference range whenever you post a number here.

No disagreement, though it depends on where somebody is starting from, and this thread has been assuming a starting point nobody stated.

BethLabQueen said:

Worth stating the units and the reference range whenever you post a number here.

This answered a question I did not know how to ask. Sending this to two other people who asked me the same thing last week.